FIELD: chemistry.
SUBSTANCE: invention can be used in chemical industry. Method of processing titanium diboride material involves chlorination of titanium diboride material with gaseous chlorine to produce titanium-containing product and boron-containing product. At least one of titanium-containing product and boron-containing product contains at least one impurity. Method includes purification by distillation of titanium-containing product and boron-containing product to a degree sufficient to reduce concentration of at least one impurity. Titanium diboride is obtained by reaction between titanium-containing and boron-containing product. Titanium diboride can be obtained by oxidation of titanium-containing product and boron-containing product to titanium dioxide and boron oxide and subsequent carbothermal reaction between titanium dioxide and boron oxide. Titanium diboride can also be obtained by exposing titanium-containing product and boron-containing product to a gas reducing agent, such as hydrogen.
EFFECT: invention enables to obtain purified titanium diboride from wastes or waste articles containing TiB2.
16 cl, 8 dwg, 2 ex
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Authors
Dates
2017-08-28—Published
2013-06-05—Filed