METHOD OF OBTAINING POROUS COORDINATION POLYMER MOF-177 Russian patent published in 2017 - IPC C07F3/06 B01J20/26 B01J20/30 B01J32/00 

FIELD: chemistry.

SUBSTANCE: method involves mixing salt-zinc acetate and 1,3,5-trifenilbenzol-p,p,p'-tricarboxylic acid, made mass ratio of 2.5:1-4.5, in the presence of the solvent, in sufficient quantity to dissolve the reactants, the subsequent heating the reaction mixture obtained under the influence of microwave radiation and allocation of the target product. As a solvent, a mixture of water and polar organic cosolvent, taken at a weight ratio of 1:1-4, is used, respectively. The process is carried out at atmospheric pressure and heating the reaction mixture to a temperature of 120-140°C under the influence of microwave radiation with power up to 200 Watts.

EFFECT: invention simplifies technology polymer MOF-177, improving the performance of the process while maintaining high output.

2 cl, 1 tbl, 5 ex