FIELD: metallurgy.
SUBSTANCE: method involves reduction of oxide compound powder of valve metal with pairs of magnesium or calcium by heating in inert atmosphere, heat treatment of reduction products is carried out at temperature of 1000-1500°C for 0.5-2 hours, acid leaching of magnesium or calcium oxide from reduction products. Production of valve metal powder, in particular, tantalum or niobium with oxygen content not more than 2.8 mg/m2 with specific surface area value 0.94-5.42 m2/g.
EFFECT: possibility for using the powder as a capacitor.
6 cl, 1 tbl, 8 ex
Authors
Dates
2018-03-29—Published
2016-06-27—Filed