APPLICATION OF SYNTHETIC ZEOLITES FOR INCREASING SELECTIVITY IN THE PRODUCTION OF 4,4-DIMETHYL-1,3-DIOXANE (OPTIONS) Russian patent published in 2018 - IPC C07D319/06 B01J29/70 

Abstract RU 2668276 C2

FIELD: biochemistry.

SUBSTANCE: invention relates to basic organic and petrochemical synthesis and can be used for producing 4,4-dimethyl-1,3-dioxane by condensation of isobutylene and formaldehyde. Proposed are synthetic zeolites of general formula Na12[(AlO2)12(SiO2)12]xH2O grade NaA with pore diameter 4 Å or Ca4,5Na3[(AlO2)12(SiO2)12]xH2O grade CaA with pore diameter 5 Å as heterogeneous cocatalysts. Synthesis of DMD is carried out in the presence of phosphoric acid, taken as the basic acid catalyst.

EFFECT: technical result is the increased selectivity in the production of 4,4-dimethyl-1,3-dioxane.

3 cl, 3 ex, 1 tbl

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RU 2 668 276 C2

Authors

Talipov Rifkat Faatovich

Vakulin Ivan Valentinovich

Tukhvatshin Vadim Salavatovich

Ovchinnikov Grigorij Andreevich

Nasyrov Ildus Shajkhitdinovich

Ishmuratov Gumer Yusupovich

Gorskikh Valentina Andreevna

Dates

2018-09-28Published

2016-09-12Filed