EFFECT: organic synthesis.
SUBSTANCE: invention relates to the use of carbon nanotubes with a pore diameter of 7-11 as a heterogeneous co-catalyst in the production of 4,4-dimethyl-1,3-dioxane (DMD) by condensation of tert-butanol and formaldehyde. In this case, the synthesis of DMD is carried out in the presence of phosphoric acid, taken as a base acid catalyst.
EFFECT: increase in the selectivity of the formation of 4,4-dimethyl-1,3-dioxane.
1 cl, 1 tbl, 2 ex
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Authors
Dates
2022-01-18—Published
2021-03-16—Filed