FIELD: chemistry.
SUBSTANCE: invention relates to a process for the preparation of 1,1-dibromo-1-fluoroethane, comprising step A of reacting 1,1-dibromoethylene with hydrogen fluoride in the presence of an amine to obtain 1,1-dibromo-1-fluoroethane. Amount of amine is within the range of 1 to 30% (w / w) relative to hydrogen fluoride.
EFFECT: technical result is a simple and stable preparation of 1,1-dibromo-1-fluoroethane with improved yield.
4 cl, 8 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF SYNTHESIS OF 1,1-DICHLORO-1-FLUOROETHANE AND A METHOD OF 1,1-DICHLOROETHYLENE CONTENT DECREASE | 1990 |
|
RU2024474C1 |
| METHOD FOR PRODUCING DIFLUOROMETHYLENE COMPOUND | 2017 |
|
RU2759911C2 |
| FLUORINATION OF ACRYLATE ESTERS AND DERIVATIVES | 2012 |
|
RU2662159C1 |
| FLUORIDATION OF ESTERS OF ACRYLIC ACID AND DERIVATIVES THEREOF | 2018 |
|
RU2697581C1 |
| METHOD OF PRODUCING HEXAFLUORO-1,3-BUTADIENE AND INTERMEDIATE COMPOUND THEREOF | 2021 |
|
RU2815788C1 |
| FLUORINATION OF ACRYLATE ESTERS AND DERIVATIVES | 2012 |
|
RU2619108C2 |
| METHOD FOR PRODUCTION OF 1,1-DICHLOR-1-FLUOROETHANE | 1989 |
|
RU2054407C1 |
| METHOD OF OBTAINING 4-AMINO-5-FLUORO-3-HALOGEN-6-(SUBSTITUTED)PICOLINATES | 2012 |
|
RU2545074C1 |
| 0 |
|
SU365895A1 | |
| METHOD FOR PRODUCING 4-AMINO-5-FLUORO-3-HALOGEN-6- (SUBSTITUTED) PYCOLINATES | 2013 |
|
RU2632203C2 |
