METHOD OF PRODUCING 2-PERFLUOROMETHYLPENTENE-2 Russian patent published in 2019 - IPC C07C21/18 C07C17/26 B01J27/12 

Abstract RU 2686316 C1

FIELD: pharmaceuticals.

SUBSTANCE: invention relates to a method of producing 2-perfluoromethylpentene-2 by dimerisation of hexafluoropropene, which is fed 0.15–0.5 l/min at temperature of 200–350 °C per catalyst. Dimerisation is carried out at excess pressure of 100–700 kPa, and said catalyst is active carbon with applied CsF, which is pre-dried in a reactor at temperature of 105–120 °C under vacuum, and then at temperature 250–350 °C, with alternation of nitrogen blowing and evacuation, absolute pressure in both cases is 66.5–1.33 kPa.

EFFECT: obtaining 2-perfluoromethylpentene-2 with output of more than 95 % and selectivity of more than 97 %, simple process technology.

1 cl, 4 tbl, 46 ex

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RU 2 686 316 C1

Authors

Barabanov Valerij Georgievich

Bispen Tatyana Alekseevna

Mitichuk Vadim Dmitrievich

Maslennikov Igor Georgievich

Moldavskij Dmitrij Dmitrievich

Dates

2019-04-25Published

2018-12-06Filed