FIELD: chemistry.
SUBSTANCE: invention relates to a method for purifying perfluoroethylisopropyl ketone (PFEC) used as a fire extinguishing agent, a solvent, a medium for carrying out chemical and biochemical processes. The method includes the excretion of hexafluoropropane Dimer from "raw" PFEC and subsequent rectification, while excretion is carried out by treatment with gaseous fluorine, then washed with aqueous sodium bicarbonate, dried with zeolite and the resulting mixture is rectified.
EFFECT: method allows to obtain perfluoroethylisopropyl ketone of the required purity.
1 dwg, 4 ex
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Authors
Dates
2017-12-20—Published
2016-02-17—Filed