METHOD OF PRODUCING A DIPOTASSIUM SALT OF THE 2,4-DI(α-METHOXYETHYL)DEUTEROPORPHYRIN IX ACETYLACETONATE YTTERBIUM COMPLEX Russian patent published in 2019 - IPC C07F5/00 C07D487/22 

Abstract RU 2697418 C1

FIELD: chemistry.

SUBSTANCE: present invention relates to chemistry of lanthanide complexes of porphyrins, in particular, to a method of producing a dipotassium salt of an ytterbium complex of 2,4-di(α-methoxyethyl)deuteroporphyrin IX of acetylacetonate. Method comprises reacting a disodium salt of 2,4-di(α-methoxyethyl)deuteroporphyrin IX with ytterbium acetylacetonate in 1,2,4-trichlorobenzene, recovering the obtained ytterbium complex of 2,4-di(α-methoxyethyl)deuteroporphyrin IX of acetylacetonate from the reaction mass by precipitation with an aliphatic hydrocarbon solvent, followed by conversion of the complex to a dipotassium salt and chromatographic purification thereof.

EFFECT: present invention allows to increase technical and economic indices of the process and output of the end product.

1 cl, 2 dwg, 4 ex

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RU 2 697 418 C1

Authors

Shchelkunova Anastasiya Evgenevna

Rumyantseva Valentina Dmitrievna

Ponomarev Gelij Vasilevich

Chernyshev Valerij Petrovich

Karakotov Salis Dobaevich

Dates

2019-08-14Published

2019-05-29Filed