FIELD: technological processes.
SUBSTANCE: invention relates to a method of producing a suspension of silver used in production of aseptic agents and textile products. Method includes the following steps: obtaining a suspension of silver oxalate with concentration of silver oxalate particles of 5–55 g/l by dispersing silver oxalate in a dispersed medium at a temperature of -5 to 0 °C, containing a mixture of a stabilizer and an anhydrous solvent containing ethylene glycol and ethyl alcohol in ratio of 1:1, wherein the content of the stabilizer in the dispersion medium is 1 wt%; obtaining a suspension containing silver nanoparticles and a dispersion medium containing a mixture of a stabilizer and an anhydrous solvent containing ethylene glycol and ethyl alcohol in ratio of 1:1, wherein the content of the stabilizer in the dispersion medium is 1 wt%, and concentration of silver nanoparticles of 5–50 g/l, by adding to obtained suspension of silver oxalate solution of diethylamine in ethyl alcohol, containing 80 wt% of diethylamine and subsequent precipitation with formic acid.
EFFECT: increase in suspension stability time at which no precipitate containing silver particles precipitates in it, and increased time of increasing silver particles size.
1 cl, 4 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PRODUCING ULTRA-HIGH MOLECULAR WEIGHT POLYETHYLENE POWDER MODIFIED BY SILVER NANOPARTICLES | 2016 |
|
RU2631567C1 |
METHOD OF PRODUCING ULTRA-HIGH MOLECULAR POLYETHYLENE (UHMPE) IMPREGNATED BY SILVER NANOPARTICLES | 2016 |
|
RU2644907C1 |
METHOD OF PRODUCING COLLOIDAL SILVER NANOPARTICLES | 2015 |
|
RU2602534C2 |
METHOD FOR OBTAINING NANO-SIZED SILVER PARTICLES | 2022 |
|
RU2802603C1 |
NANOSILVER COLLOIDAL SOLUTION AND PREPARATION METHOD THEREOF | 2016 |
|
RU2618303C1 |
METHOD OF PRODUCING CONCENTRATES OF ZEROVALENT METAL DISPERSIONS WITH ANTISEPTIC PROPERTIES | 2010 |
|
RU2445951C1 |
METHOD OF PRODUCING HIGHLY CONCENTRATED ORGANOSOL OF SILVER NANOPARTICLES | 2023 |
|
RU2821522C1 |
METHOD OF PRODUCING SILVER NANOPARTICLES | 2011 |
|
RU2448810C1 |
METHOD FOR ANTIBACTERIAL TREATMENT OF YEAST | 2015 |
|
RU2584603C1 |
COLLOIDAL SOLUTION OF NANOSILVER IN ETHYLENE-GLYCOL AND METHOD OF ITS PRODUCTION | 2015 |
|
RU2610197C2 |
Authors
Dates
2019-08-21—Published
2018-12-04—Filed