METHOD OF PRODUCING A ZINC-PICOLINIC ACID COORDINATION COMPOUND Russian patent published in 2020 - IPC C07F3/06 C25B3/12 

Abstract RU 2711449 C1

FIELD: chemistry.

SUBSTANCE: invention relates to synthesis of chemicals, specifically to a method of producing a zinc-picolinic acid coordination compound. Method involves reaction of a metal ion with a ligand in the medium of a three-component aqueous organic solvent with subsequent separation of the residue. Solvent used is a system of acetonitrile : ethanol : water with volume ratio of components of 13:6:1, the reaction is carried out by electrolysis of a solution containing picolinic acid, with zinc electrodes and potassium chloride as a background electrolyte, wherein the weight ratio of acetonitrile : ethanol : water : picolinic acid : electrolyte is 51.19:23.68:5.00:1.00:0.05, the density of direct current is equal to 3–5 mA/cm2.

EFFECT: technical result is obtaining a coordination compound of zinc with picolinic acid in one step and with shorter time costs.

1 cl, 4 dwg, 3 tbl, 1 ex

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RU 2 711 449 C1

Authors

Zelenov Valerij Igorevich

Andrijchenko Elena Olegovna

Bovyka Valentina Evgenevna

Ekotova Elizaveta Olegovna

Dates

2020-01-17Published

2019-09-27Filed