FIELD: organic chemistry.
SUBSTANCE: invention relates to synthetic organic chemistry, namely to a method for producing melamine borate. The method for producing melamine borate is carried out in a paddle mixer by mixing boric acid and melamine, while melamine is mixed with boric acid at a temperature of 20 to 100°C for 20-30 minutes, then ammonium borate is added and the mixture is heated to a temperature of 200-300°C and kept for 30-90 minutes at a molar ratio of melamine/boric acid/ammonium tetraborate 1:0.25-1.6:0.25-1, followed by cooling and grinding.
EFFECT: proposed method makes it possible to produce melamine borate with a yield of at least 75%, with a decomposition start temperature above 300°C and a residual mass after calcination at 500°C of at least 40%, using a single apparatus, without the release of intermediate reaction products, as well as high water and energy consumption.
1 cl, 1 dwg, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING ADDUCT OF PHOSPHORIC AND BORIC ACIDS | 2021 |
|
RU2767855C1 |
| METHOD FOR OBTAINING MELAMINE CYANURATE | 2021 |
|
RU2758252C1 |
| METHOD FOR OBTAINING MELAMINE POLYPHOSPHATE | 2021 |
|
RU2758253C1 |
| METHOD FOR PREPARING MELAMINE ADDUCT WITH ACID | 2005 |
|
RU2292341C1 |
| EPOXY COMPOSITION FOR PRODUCING INTUMESCENT FIRE-RETARDANT COATINGS | 2024 |
|
RU2826386C1 |
| METHOD FOR PRODUCING CRYSTALLINE MEL-TYPE ZEOLITE AND MEL-TYPE ZEOLITE | 2023 |
|
RU2805757C1 |
| ALUMINA SUPPORT, METHOD FOR MAKING ALUMINA SUPPORT AND METHOD FOR MAKING DEHYDROGENATION CATALYST OF C-C PARAFFIN HYDROCARBONS ON THIS SUPPORT | 2007 |
|
RU2350594C1 |
| COMPOSITION FOR PRODUCING FIRE- AND HEAT-PROTECTIVE COATINGS | 2024 |
|
RU2826372C1 |
| TRANSPARENT GEL-POLYMER ELECTROLYTES OF HIGH CONDUCTIVITY BASED ON TRIAZINE COPOLYMERS | 2020 |
|
RU2818669C1 |
| COMPOSITION FOR FIRE-RESISTANT FOAMED POLYURETHANE | 2019 |
|
RU2714917C1 |
