FIELD: chemistry.
SUBSTANCE: invention relates to a method for producing bis(2,2,3,3-tetrafluoropropyl)carbonate using sequential treatment of a mixture of 2,2,3,3-tetrafluoropropanol-1 and benzene with titanium (IV) alkoxide and diphenyl carbonate followed by distillation of bis(2,2,3,3-tetrafluoropropyl)carbonate at atmospheric pressure.
EFFECT: obtaining bis(2,2,3,3-tetrafluoropropyl)carbonate in a simple and effective way using minimal amounts of commercially available and non-toxic reagents.
1 cl, 3 ex
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Authors
Dates
2022-01-25—Published
2021-01-25—Filed