METHOD FOR OBTAINING N,N-DIMETHYL-4-BIPHENYLAMINE AND ITS DERIVATIVES Russian patent published in 2023 - IPC C07C209/68 C07C211/48 C07C227/16 C07C229/52 

Abstract RU 2794095 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method for producing N,N-dimethyl-4-biphenylamine and its derivatives of the General formula (R1)Ph-Ph(R2)-N(CH3)2, where R1-H, n-SOOSH3, R2-H, o-CH3. The method is the interaction of N,N-dimethylaminophenyldiazenilaryl of the general formula (R1)Ph-N=N-Ph(R2)-N(CH3)2, where R1 is H, n-COOCH3, R2 is H, o-CH3, tetracyanoethylene and methanol under the action of ultrasound at a frequency of 90–100 Hz and a temperature of 35-40°C.

EFFECT: use of affordable inexpensive reagents, the absence of catalysts and bases, one-stage and reduced reaction time.

1 cl, 3 ex

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RU 2 794 095 C1

Authors

Nasakin Oleg Evgenevich

Ivanova Elizaveta Sergeevna

Lyalin German Semenovich

Eremkin Aleksej Vladimirovich

Vishnevetskaya Darina Aleksandrovna

Lodochnikova Olga Aleksandrovna

Dates

2023-04-11Published

2022-11-01Filed