FIELD: nano-optics.
SUBSTANCE: invention relates to nano-optics and can be used in designing chemoptical sensors, for example, for optical detection of vapours of toxic or hazardous chemical compounds at chemical industry enterprises. Method of producing a chemooptical sensor in form of 2D ZnTBAPy layer involves layering the MOF in a polar solvent by multiple freezing-thawing, wherein freezing is carried out in liquid nitrogen at a temperature of -196 °C and is characterized by the fact that the MOF freezing-thawing process is repeated 8-12 times, solvent is DMF, methanol or ethanol, and thawing is carried out in water heated from 70 to 85 °C. 2D ZnTBAPy is used in the form of a powder, the particles of which are dried before delamination, mixed with dimethylformamide and after the last thawing, a conclusion is made on obtaining a sensor.
EFFECT: obtaining thin layers of high surface area with high level of optical response when detecting toxic vapours.
1 cl, 2 ex
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Authors
Dates
2024-11-12—Published
2024-03-12—Filed