FIELD: organic chemistry. SUBSTANCE: synthesis is carried out by reaction of corresponding steroid and ethylene glycol following by treatment with gaseous tritium in the presence of Pd-catalyst in organic solvent and splitting off of ethylene glycol protected group in acid medium. Yield of the end products is 67% , molar activity is 1.97 PBq/mole, radiochemical purity is 95-97% . EFFECT: high molar activity of product. 1 tbl
| Title |
Year |
Author |
Number |
| METHOD OF SYNTHESIS OF TETRAMETHYL-4-HYDROXY(AMINO)PIPERIDINES OR AMINODODECANOIC ACID LABELED WITH TRITIUM |
1986 |
- Shevchenko V.P.
- Potapova A.V.
|
SU1432969A3 |
| 5α- AND 5β-[4,5-α]-PREGNANE-3,20-DIONES HIGHLY LABELED WITH TRITIUM AND METHOD OF THEIR DETERMINATION IN BLOOD PLASMA |
2001 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Kareva E.N.
- Podval'Njuk V.V.
- Ovchinnikova E.V.
|
RU2183123C1 |
| METHOD OF SYNTHESIS OF PROSTAGLANDINS TYPE e, OR THEIRS DERIVATIVES TYPE A, B, F, OR METHYL ESTERS OF PROSTAGLANDIN TYPE 1 MULTIPLE LABELED WITH TRITIUM |
1988 |
- Lazurkina T.Ju.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Shevchenko V.P.
- Shram S.I.
|
SU1646252A3 |
| METHOD OF PREPARING QUATERNARY AMINE SALTS CONTAINING TRITIUM LABELLED AROMATIC RADICAL AT NITROGEN ATOM |
1995 |
- Shevchenko V.P.
- Mjasoedov N.F.
|
RU2089532C1 |
| METHOD OF SYNTHESIS OF 4-ETHYL-2,6,7-TRIOXA-1-PHOSPHOBICYCLO-[2,2,2]-OCTANE-1-OXIDE HIGHLY LABELED WITH TRITIUM OR DEUTERIUM AT ETHYL RADICAL |
1995 |
- Mjasoedov N.F.
- Shevchenko V.P.
- Faradzheva S.V.
- Nagaev I.Ju.
|
RU2108337C1 |
| 2-METHYL-3-PHYTHYL-1,4-NAPHTHOQUINONE HIGHLY LABELED WITH TRITIUM |
2001 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2190591C1 |
| ETHYLACETAMIDE HIGHLY LABELED WITH TRITIUM |
2000 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2183610C1 |
| [H]-7-CHLORO-1,3-DIHYDRO-1-METHYL-5-PHENYL-2H-1,4- BENZDIAZEPINE-2-ONE HIGH-LABELED WITH TRITIUM AND METHOD FOR ITS PREPARING |
2003 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Shevchenko K.V.
|
RU2247116C2 |
| METHOD OF SYNTHESIS OF PROLINE HIGH-LABELED WITH TRITIUM |
1986 |
- Dorokhova E.M.
- Zolotarev Ju.A.
- Kozik V.S.
- Mjasoedov N.F.
|
SU1432968A3 |
| 2-METHYL-4-(4-METHYL-1-PIPERAZINYL)-10H-THIENO-[2,3-B][1,5]BENZODIAZEPINE HIGH-LABELED WITH TRITIUM |
2001 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Zozulja A.A.
- Kost N.V.
- Khomjakova A.V.
|
RU2185383C1 |
