FIELD: organic chemistry, basic monoamino acids. SUBSTANCE: corresponding ketone or oxime of piperidine or acid nitrile is subjected for solid-phase reduction with gaseous tritium at 80 C (for nitriles and ketones) and at 95-105 C (for oximes) in the presence of catalyst Rh/C. Method ensures to prepare the end product showing molar radioactivity 1.6-4.8 PBq/mole (0.12 PBq/mole by known method). EFFECT: enhanced molar radioactivity of product. 2 tbl
| Title |
Year |
Author |
Number |
| METHOD OF PREPARING QUATERNARY AMINE SALTS CONTAINING TRITIUM LABELLED AROMATIC RADICAL AT NITROGEN ATOM |
1995 |
- Shevchenko V.P.
- Mjasoedov N.F.
|
RU2089532C1 |
| METHOD OF SYNTHESIS OF PROSTAGLANDINS TYPE e, OR THEIRS DERIVATIVES TYPE A, B, F, OR METHYL ESTERS OF PROSTAGLANDIN TYPE 1 MULTIPLE LABELED WITH TRITIUM |
1988 |
- Lazurkina T.Ju.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Shevchenko V.P.
- Shram S.I.
|
SU1646252A3 |
| [H]-7-CHLORO-1,3-DIHYDRO-1-METHYL-5-PHENYL-2H-1,4- BENZDIAZEPINE-2-ONE HIGH-LABELED WITH TRITIUM AND METHOD FOR ITS PREPARING |
2003 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Shevchenko K.V.
|
RU2247116C2 |
| METHOD OF SYNTHESIS OF 4-ETHYL-2,6,7-TRIOXA-1-PHOSPHOBICYCLO-[2,2,2]-OCTANE-1-OXIDE HIGHLY LABELED WITH TRITIUM OR DEUTERIUM AT ETHYL RADICAL |
1995 |
- Mjasoedov N.F.
- Shevchenko V.P.
- Faradzheva S.V.
- Nagaev I.Ju.
|
RU2108337C1 |
| METHOD OF SYNTHESIS OF 3′, 4′, -H - 16α, 17α-CYCLOHEXANOPREGN-4-EN-3, 20-DIONE LABELED WITH TRITIUM |
1986 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Kamernitskij A.V.
- Levina I.S.
- Kulikova L.E.
- Fanchenko N.D.
- Minina L.S.
|
SU1387385A3 |
| METHOD OF SYNTHESIS OF UNSATURATED SIMPLE LIPIDS MULTIPLE-LABELED WITH TRITIUM AT DOUBLE BONDS |
1988 |
- Nagaev I.Ju.
- Shevchenko V.P.
- Mjasoedov N.F.
- Mjagkova G.I.
- Evstigneeva R.P.
|
SU1582553A3 |
| METHOD OF SYNTHESIS OF PURINE BASES LABELED WITH TRITIUM |
1986 |
- Mjasoedov N.F.
- Sidorov G.V.
- Voronkov A.L.
- Kvjatkovskij Ju.G.
- Ivan'Kova E.K.
|
SU1545504A3 |
| TRITIUM HIGHLY MARKED-(2-ANO-2-METHOXYIMINOACETYL)-3- ETHYLUREA |
1998 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2155175C2 |
| TRITIUM HIGH-LABELED DIMETHOMORPHOLINE AND METHOD OF PREPARATION THEREOF |
1998 |
- Shevchenko V.P.
- Nagaev I.Ju.
- Mjasoedov N.F.
|
RU2136672C1 |
| METHOD OF SYNTHESIS OF PROLINE HIGH-LABELED WITH TRITIUM |
1986 |
- Dorokhova E.M.
- Zolotarev Ju.A.
- Kozik V.S.
- Mjasoedov N.F.
|
SU1432968A3 |
