METHOD OF SYNTHESIS OF OCTAFLUOROPROPANE AND A REACTOR FOR ITS REALIZATION Russian patent published in 1995 - IPC

Abstract RU 2041194 C1

FIELD: chemical technology, fluorinated hydrocarbons. SUBSTANCE: synthesis is carried out by reaction of hexafluoropropylene with cobalt trifluoride at 75-450 C in two-zone vertical tube reactor with jacket and heat-exchanger in the form of cylindrical capacity with jacket. Internal walls of the latter form central cavity which is the second reaction zone. The first zone is annular cavity formed by reactor corpus walls and cylindrical capacity. In the second reaction zone ratio of cobalt difluoride and cobalt trifluoride is maintained as 1: (1-1.5). Hexafluoropropylene is fed into annular cavity at the linear rate 2.45-2.5 m/s. The end product is removed from the central cavity. EFFECT: improved method of synthesis. 3 cl, 1 dwg

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RU 2 041 194 C1

Authors

Asovich V.S.

Alekseev Ju.I.

Ivanova T.Ja.

Korolev V.L.

Maruev A.V.

Mel'Nichenko B.A.

Dates

1995-08-09Published

1992-08-07Filed