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2 200 156

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Application

2001110202/04, 2001-04-13

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Start date

2001-04-13

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Actual filing date

2001-04-13

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Published

2003-03-10

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Inventor

Khusnutdinov R.I.Atnabaeva A.M.Parfenova R.I.Muslimov Z.S.Dzhemilev U.M.Kovtunenko I.A.

(73)

Holder

Institut Neftekhimii I Kataliza An Rb I Unts Ran

METHOD OF SYNTHESIS OF 3,5-DIMETHYL-2-ETHYL-PYRIDINE Russian patent published in 2003 - IPC

Abstract RU 2200156 C2

FIELD: organic chemistry, chemical technology. SUBSTANCE: invention relates to the field of organic synthesis, namely, to method of synthesis of 3,5-dimethyl-2-ethylpyridine that can be used in synthesis of corrosion inhibitors and medicinal preparations. Method if based on heterocyclization reaction of allylamine by palladium chloride as catalyst in the mole ratio [PdCl2] : [allylamine] = [0.01-0.005] : 1, respectively. Reaction is carried out at temperature 140-160 C for 6-9 h. The yield of end product is 69%. Method differs from the known ones by the more yield of end product, more mild reaction conditions and high selectivity of process. EFFECT: improved method of synthesis, increased yield of product. 1 cl, 3 ex

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RU 2 200 156 C2

Authors

Khusnutdinov R.I.

Atnabaeva A.M.

Parfenova R.I.

Muslimov Z.S.

Dzhemilev U.M.

Kovtunenko I.A.

Dates

2003-03-10—Published

2001-04-13—Filed

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