FIELD: chemistry.
SUBSTANCE: invention relates to production of aluminium hydroxide from aluminium metal, which can be used as a modifying additive for polymer materials for producing active aluminium oxide for making extra strong and fire resistant ceramic articles, composite materials and antipyrenes. The electrochemical method of producing aluminium oxide involves anodic dissolution aluminium metal in a chlorine-containing electrolyte solution, followed by washing and thermal treatment. Anodic dissolution is carried out in a coaxial electrolysis cell with the surface area of the anode at least twice greater than that of the cathode and the precipitate is then held in the electrolyte solution. Concentration of chloride in the electrolyte solution is equal to 0.05-0.8 mol/l and anode current density is equal to 50-300 A/m2.
EFFECT: invention enables to control the phase ratio of boehmite and bayerite and obtain aluminium hydroxide nanoparticles with size in the range of 10-200 nm.
1 dwg, 2 tbl, 4 ex, 1 dwg
Title | Year | Author | Number |
---|---|---|---|
ELECTROCHEMICAL METHOD OF PRODUCING ALUMINIUM OXIDE | 2009 |
|
RU2412904C1 |
METHOD FOR PRODUCING HIGHLY DISPERSED ALUMINIUM-ZIRCONIUM OXIDE SYSTEM | 2016 |
|
RU2615513C1 |
METHOD FOR OBTAINING MODIFIED HIGHLY DISPERSED ALUMINA SYSTEM FOR TECHNICAL CERAMICS | 2021 |
|
RU2762226C1 |
METHOD OF PRODUCING FINELY DISPERSED ALUMINIUM HYDROXIDE AND ALUMINIUM OXIDE BASED THEREON | 2010 |
|
RU2465205C2 |
METHOD OF PREPARATION OF CATALYST OF PARAFFIN ISOMERIZATION BASED ON BAYERITE ALUMINIUM OXIDE | 2017 |
|
RU2669199C1 |
METHOD OF ELECTROCHEMICAL OBTAINING OF ALUMINUM OXIDE POWDERS | 2017 |
|
RU2664135C1 |
METHOD FOR ELECTROCHEMICAL COPPER RECOVERY IN HYDROCHLORIDE SOLUTION | 2004 |
|
RU2337182C2 |
METHOD OF PRODUCING LEAD HYDROXIDE | 1991 |
|
RU2006525C1 |
METHOD OF PRODUCING NANOSIZED METAL PARTICLES | 2022 |
|
RU2816468C1 |
METHOD OF PRODUCING COPPER DISPERSED PARTICLES BY ELECTROCHEMICAL METHOD | 2019 |
|
RU2708719C1 |
Authors
Dates
2011-02-27—Published
2009-07-29—Filed