METHOD OF PRODUCING 5,6-DIHYDRO-4H-BENZO[f]PYRROLO[1,2-α][1,4]DIAZEPIN-6-ONE Russian patent published in 2011 - IPC C07D243/06 C07D487/04 

Abstract RU 2425037 C1

FIELD: chemistry.

SUBSTANCE: described is a method of producing 5,6-dihydro-4H-benzo[f]pyrrolo[ 1,2-α][1,4]diazepin-6-one 1, involving moulding a pyrrolodiazepine frame as a result of reduction of nitro-groups of N-(2,5-dioxoalkyl)-2-nitrobenzamides 4, in acetic acid in the presence of iron while carrying out the reaction until boiling and holding for 60 minutes at room temperature.

EFFECT: simultaneous formation of a pyrrole and a diazepine ring, and high output of end products owing to change in the sequence and conditions of the reaction.

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RU 2 425 037 C1

Authors

Butin Aleksandr Valerianovich

Nevolina Tat'Jana Anatol'Evna

Shcherbinin Vitalij Aleksandrovich

Trushkov Igor' Viktorovich

Krapivin Gennadij Dmitrievich

Dates

2011-07-27Published

2010-01-11Filed