1-BROMOADAMANTANE SYNTHESIS METHOD Russian patent published in 2011 - IPC C07C23/18 

Abstract RU 2428408 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method for synthesis of 1-bromoadamantane of formula (1) through catalytic bromation of adamantane. The bromation agent used is bromotrichloromethane in the presence of a Mo(CO)6 catalyst at temperature 140-160°C for 5-10 hours in molar ratio [adamantane]:[BrCCl3]Mo(CO)6=100:200-300:1-3.

EFFECT: simple technology of producing the end product and high output of the product.

1 cl, 1 tbl, 2 ex

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RU 2 428 408 C2

Authors

Dzhemilev Usein Memetovich

Khusnutdinov Ravil Ismagilovich

Shchadneva Nina Alekseevna

Mukhametshina Lilija Fagimovna

Dates

2011-09-10Published

2009-06-29Filed