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2 401 828

(13)

(51)

IPC

C07C233/06(2006-01-01)

C07C231/06(2006-01-01)

(21) (22)

Application

2008138015/04, 2008-09-23

(24)

Start date

2008-09-23

(22)

Actual filing date

2008-09-23

(45)

Published

2010-10-20

(72)

Inventor

Dzhemilev Usein MemetovichKhusnutdinov Ravil IsmagilovichShchadneva Nina AlekseevnaMukhametshina Lilija Fagimovna

(73)

Holder

Uchrezhdenie Rossijskoj Akademii Nauk Institut Neftekhimii I Kataliza Ran

N-(1-ADAMANTYL)ACETAMIDE SYNTHESIS METHOD Russian patent published in 2010 - IPC C07C233/06 C07C231/06

Abstract RU 2401828 C2

FIELD: chemistry.

SUBSTANCE: invention relates to organic chemistry, specifically to a novel method for synthesis of N-(1-adamantyl)acetamide, which can be used in synthesis of scarce adamantane derivatives. The method is realised by reacting adamantane with acetonitrile in bromotrichloromethane in the presence of water under the effect of Mo(CO)₆ at 130-140°C for 2-3 hours, in molar ratio [adamantane] : [CH₃CN] : [CBrCl₃] : [Mo(CO)₆] : [H₂O] = 100 : 100-150 : 100-150 : 1-3 : 1000-2000.

EFFECT: novel N-(1-adamantyl)acetamide synthesis method.

1 cl, 8 ex, 1 tbl

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RU 2 401 828 C2

Authors

Dzhemilev Usein Memetovich

Khusnutdinov Ravil Ismagilovich

Shchadneva Nina Alekseevna

Mukhametshina Lilija Fagimovna

Dates

2010-10-20—Published

2008-09-23—Filed