METHOD OF PRODUCING 4-(1-ADAMANTYL)-1,2-DIAMINOBENZENE Russian patent published in 2012 - IPC C07C211/50 C07C209/74 

Abstract RU 2454401 C1

FIELD: chemistry.

SUBSTANCE: invention relates to an improved method of producing 4-(1-adamantyl)-1,2-diaminobenzene, which exhibits various types of biological activity. The method involves reaction of 1-bromoadamantane and o-phenylenediamine at temperature 180°C for 8 hours in molar ratio -bromoadamantane: o-phenylenediamine equal to 1:2-3.

EFFECT: method enables to obtain 4-(1-adamantyl)-1,2-diaminobenzene in a single step from readily available reactants without using highly toxic solvent with high output (55-76%).

1 dwg, 2 ex

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RU 2 454 401 C1

Authors

Novakov Ivan Aleksandrovich

Orlinson Boris Semenovich

Savel'Ev Evgenij Nikolaevich

Potaenkova Elena Aleksandrovna

Makhaeva Tat'Jana Alekseevna

Dates

2012-06-27Published

2011-02-14Filed