METHOD OF PROCESSING BIRCH BARK TO OBTAIN BETULIN AND SUBERIC ACIDS Russian patent published in 2012 - IPC C08H7/00 

Abstract RU 2460741 C1

FIELD: chemistry.

SUBSTANCE: method involves extraction of betulin from birch bark using methyl tert-butyl ether. The bark is the treated with aqueous NaOH solution. The aqueous alkaline solution discharged from the birch bark for extracting suberic acids is treated with sulphuric acid solution. Purification of betulin from impurities in an organic extract is carried out via concentration followed by hot washing with NaOH solution and then with water, while simultaneously distilling residual methyl tert-butyl ether from the betulin. The method enables to obtain betulin and suberic acids without additional purification steps.

EFFECT: environmental safety and cost effectiveness.

2 ex

Similar patents RU2460741C1

Title Year Author Number
METHOD OF PROCESSING BIRCH BARK TO OBTAIN BETULIN AND SUBERIC ACIDS 2016
  • Popov Sergej Aleksandrovich
  • Kozlova Lyubov Pavlovna
  • Kornaukhova Lyubov Mikhajlovna
  • Shults Elvira Eduardovna
RU2620814C1
METHOD FOR PRODUCING BETULONIC ACID 2014
  • Popov Sergej Aleksandrovich
  • Kozlova Ljubov' Pavlovna
  • Kornaukhova Ljubov' Mikhajlovna
  • Shpatov Aleksandr Vladimirovich
RU2568881C1
METHOD OF PRODUCING BETULIN 28-HEMISUCCINATE 2010
  • Popov Sergej Aleksandrovich
  • Kozlova Ljubov' Pavlovna
  • Kornaukhova Ljubov' Mikhajlovna
  • Tolstikov Genrikh Aleksandrovich
RU2435779C1
METHOD OF PRODUCING BETULIN 2013
  • Mal'Chikov Evgenij Leonidovich
  • Kislitsyn Aleksej Nikolaevich
RU2524778C1
METHOD FOR COMPLEX PROCESSING OF BIRCH BARK 2016
  • Kuznetsov Boris Nikolaevich
  • Sudakova Irina Gennadevna
  • Kuznetsova Svetlana Alekseevna
  • Grishechko Lyudmila Ivanovna
  • Skvortsova Galina Pavlovna
  • Veprikova Evgeniya Vladimirovna
  • Levdanskij Vladimir Aleksandrovich
RU2618892C1
METHOD FOR CHEMICAL PROCESSING OF BIRCH BARK WITH EXTRACTION OF SUCH PRODUCTS AS BETULIN AND SUBERIN 2010
  • Mal'Chikov Evgenij Leonidovich
  • Lekanova Anastasija Evgen'Evna
  • Fomenko Evgenij Vladimirovich
RU2439093C1
METHOD FOR BETULIN ISOLATION FROM BIRCH BARK 2005
  • Taraban'Ko Valerij Evgen'Evich
  • Chernjak Mikhail Jur'Evich
  • Kuznetsov Boris Nikolaevich
  • Taraban'Ko Nikolaj Valer'Evich
RU2286349C1
METHOD FOR PREPARING BETULIN 2004
  • Junusov Marat Sabirovich
  • Komissarova Natalija Grigor'Evna
  • Belenkova Natal'Ja Gennad'Evna
RU2270201C1
METHOD FOR PRODUCING ACTIVATED CARBON 2015
  • Mikova Nadezhda Mikhajlovna
  • Chesnokov Nikolaj Vasilevich
  • Drozdov Vladimir Anisimovich
RU2582132C1
METHOD FOR PREPARING BETULIN AND LUPEOL 2004
  • Junusov Marat Sabirovich
  • Komissarova Natalija Grigor'Evna
  • Belenkova Natal'Ja Gennad'Evna
RU2270202C1

RU 2 460 741 C1

Authors

Popov Sergej Aleksandrovich

Kozlova Ljubov' Pavlovna

Kornaukhova Ljubov' Mikhajlovna

Shpatov Aleksandr Vladimirovich

Shul'Ts Ehl'Vira Ehduardovna

Tolstikov Genrikh Aleksandrovich

Dates

2012-09-10Published

2011-04-05Filed