METHOD OF OBTAINING 1-ALKYNYL ADAMANTANES Russian patent published in 2014 - IPC C07C13/615 C07C2/86 C07C6/08 B01J23/08 C07C1/20 C07C1/32 C07C11/22 

Abstract RU 2507189 C1

FIELD: chemistry.

SUBSTANCE: invention relates to method of obtaining 1-alkynyl adamantanes from derivatives of adamantine and acetylene compounds with catalysis with Lewis acid, taken in equimolar amounts. Method is characterised by the following: as initial components used are 1-adamantanol and 1-alkene or 1-trimethylsilylalkene, which are heated at temperature of 1,2-dichloroethane boiling in presence of 5 molar percent of gallium triflate as Lewis acid until initial compounds are fully consumed.

EFFECT: application of claimed method makes it possible to obtain target compound from commercially available initial compounds with good output of target product.

1 cl, 1 tbl, 10 ex

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RU 2 507 189 C1

Authors

Konshin Valerij Viktorovich

Turmasova Anna Alekseevna

Konshina Dzhamilja Naibovna

Dates

2014-02-20Published

2012-07-05Filed