FIELD: chemistry.
SUBSTANCE: present invention relates to the method of producing 1-adamantyl-acetaldehyde, used as a valuable intermediate product for synthesis of bioactive substances and functional organic materials. The method comprises a catalytic reaction between 1-adamantanol and vinyl acetate as an unsaturated compound. Vinyl acetate, 2.5-fold molar excess relative to 1-adamantanol; the reaction is caried out for 2 hours in dichloroethane at dichloroethane boiling point, indium tribromide is used as a catalyst, 5 mole %.
EFFECT: target product produced using a simple process and readily available raw materials.
2 tbl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING 1-ADAMANTYL FERROCENE | 2018 |
|
RU2691998C1 |
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|
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| METHOD FOR OBTAINING ACETYLENE KETONES | 2017 |
|
RU2641697C1 |
| METHOD FOR PRODUCING 4-(1-ADAMANTYL)ANILINE | 2014 |
|
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| METHOD OF PRODUCING 4-(1-ADAMANTYL)ANILINE | 2014 |
|
RU2549902C1 |
