FIELD: chemistry.
SUBSTANCE: method includes mixing solutions of calcium salts and a phosphate, settling, filtering, washing from the mother solution and drying. The starting components used are calcium nitrate tetrahydrate and anhydrous disubstituted ammonium phosphate; the ratio of concentration of reagents (Ca/P) is equal to 1.00 or 1.70; the concentration of Ca(NO3)2 in the reaction system varies in the range of 0.010-0.050 mol/l; content of (NH4)2HPO4 is calculated based on the selected ratio of Ca/P and concentration of Ca(NO3)2; pH is kept at 5.00-6.50. After precipitation, the obtained solid phase is held under the mother solution for 2 days at 22-25°C, filtered, washed with distilled water and dried at 80°C until complete removal of non-chemically bound water.
EFFECT: obtaining powdered material with content of components variable in a wide range.
1 tbl, 2 dwg, 2 ex
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Authors
Dates
2015-04-10—Published
2014-03-20—Filed