ELECTROCHEMICAL METHOD OF OBTAINING CYCLOHEXANETHIOL IN ORGANIC SOLVENTS Russian patent published in 2015 - IPC C07C319/04 C07C321/22 C25B3/00 

Abstract RU 2550141 C1

FIELD: chemistry.

SUBSTANCE: invention relates to an electrochemical method of obtaining cyclohexanethiol in organic solvents. The method includes the interaction of cyclohexane with hydrogen sulphide under atmospheric pressure, with carrying out a one-stage reaction of cyclohexane with hydrogen sulphide under electrolysis conditions with the potential of hydrogen sulphide oxidation in an organic solvent, in which supporting electrolyte is placed, without the application of a catalyst or a specific reagent at a temperature of the process of 20-25°C.

EFFECT: application of the claimed method makes it possible to obtain the target product with high selectivity and relatively large output under atmospheric pressure without the application of the specific catalyst.

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RU 2 550 141 C1

Authors

Berberova Nadezhda Titovna

Kudrjavtsev Daniil Aleksandrovich

Shinkar' Elena Vladimirovna

Aref'Ev Jaroslav Borisovich

Pashchenko Konstantin Petrovich

Dates

2015-05-10Published

2013-10-29Filed