FIELD: measurement equipment.
SUBSTANCE: invention relates to analytical atomic spectrometry and can be used in a spectral analysis for an express method of determining an element composition of a substance. The method is based on action of two subsequent collinear laser pulses directed to one point of a sample surface; with that, a value of inter-pulse delay is chosen equal to the time for which at single-pulse action on the sample there achieved is maximum signal-to-noise ratio. Radiation of laser plasma after action of the second pulse is recorded by means of a spectrograph and a gated electronic-optic digital chamber, and then, quantitative determination of trace components of the sample is performed via emission atomic and ionic lines.
EFFECT: invention provides improvement of sensitivity and express properties of the analysis at interaction of two laser radiation pulses per sample.
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR LASER SPARK SPECTRAL ANALYSIS FOR DETERMINATION OF SUBSTANCE SAMPLE ULTIMATE COMPOSITION | 2010 |
|
RU2436070C1 |
METHOD OF LASER-SPARK EMISSION DETERMINATION OF ARSENIC IN FOOD RAW MATERIAL AND FOODSTUFF | 2013 |
|
RU2531026C1 |
METHOD FOR LASER-SPARK EMISSION DETERMINATION OF BERYLLIUM IN METAL ALLOYS AND POWDERS | 2015 |
|
RU2583858C1 |
METHOD FOR LASER-SPARK EMISSION DETERMINATION OF LANTHANUM, CERIUM, PRASEODYMIUM AND NEODYMIUM IN METAL ALLOYS AND POWDERS | 2013 |
|
RU2548584C2 |
METHOD FOR LASER-SPARK EMISSION DETERMINATION OF TOXIC ELEMENTS IN FOOD RAW MATERIAL AND PRODUCTS | 2011 |
|
RU2483294C2 |
METHOD OF LAYER-BY-LAYER LASER SPECTRAL ANALYSIS | 1997 |
|
RU2110777C1 |
METHOD OF DETERMINING WEIGHT RATIO OF OXYGEN IN METAL POWDERS | 2013 |
|
RU2530483C1 |
MODE OF LASER-SPARK SPECTRAL ANALYSIS | 2006 |
|
RU2300094C1 |
METHOD FOR NUCLEAR-ABSORPTION SPECTRAL ANALYSIS OF ELEMENTARY COMPOSITION OF MATERIAL AND DEVICE WHICH IMPLEMENTS SAID METHOD | 1998 |
|
RU2157988C2 |
METHOD OF DETERMINING CONTENT OF METALS IN LIQUID SAMPLES AND DEVICE FOR IMPLEMENTATION THEREOF | 2018 |
|
RU2701452C1 |
Authors
Dates
2015-05-10—Published
2013-09-11—Filed