METHOD OF PRODUCING 1-ADAMANTYL ISOTHIOCYANATE Russian patent published in 2015 - IPC C07C331/26 

Abstract RU 2551682 C1

FIELD: chemistry.

SUBSTANCE: method includes reacting an adamantane derivative with an isothiocyanate derivative while boiling in a solvent medium and then extracting the reaction product. The adamantane derivative used is 1,3-dehydroadamantane and the isothiocyanate derivative is a solution of isothiocyanic acid solution in diethyl ether prepared in advance. The reaction is carried out in a medium of diethyl ether for 3 hours in molar ratio of 1,3-dehydroadamantane:isothiocyanic acid:diethyl ether=1:1.5:20.

EFFECT: method enables to obtain a 1-adamantyl isothiocyanate in mild conditions with high output.

1 ex

Similar patents RU2551682C1

Title Year Author Number
METHOD OF PRODUCING 1-ADAMANTYL ISOCYANATE 2014
  • Butov Gennadij Mikhajlovich
  • Mokhov Vladimir Mikhajlovich
  • Burmistrov Vladimir Vladimirovich
  • Pitushkin Dmitrij Andreevich
RU2551681C1
METHOD OF PRODUCING ADAMANTYL-CONTAINING ISOTHIOCYANATES 2015
  • Butov Gennadij Mikhajlovich
  • Saad Karim Ramez
  • Burmistrov Vladimir Vladimirovich
  • Pitushkin Dmitrij Andreevich
RU2599993C1
METHOD OF PRODUCING 3-IODO-1-PERFLUOROALKYLADAMANTANES 2019
  • Gladkikh Boris Pavlovich
  • Mokhov Vladimir Mikhajlovich
  • Butov Gennadij Mikhajlovich
RU2700771C1
METHOD OF PRODUCING 1-ADAMANTYLHYDROPEROXIDE 2011
  • Butov Gennadij Mikhajlovich
  • Mokhov Vladimir Mikhajlovich
  • Ledenev Sergej Mikhajlovich
  • Terent'Ev Aleksandr Olegovich
RU2471780C1
METHOD OF OBTAINING N,N-DIALKYL-SUBSTITUTED AMIDES OF ADAMANTYLALKYLCARBOXYLIC ACIDS 2007
  • Butov Gennadij Mikhajlovich
  • Mokhov Vladimir Mikhajlovich
RU2348611C1
METHOD OF OBTAINING ADAMANTYL CONTAINING DERIVATIVES OF 1,4-DIKETONES 2006
  • Butov Gennadij Mikhajlovich
  • Kunaev Roman Uazerovich
  • Parshin Gleb Jur'Evich
  • Mokhov Vladimir Mikhajlovich
RU2330013C1
METHOD OF PRODUCING ADAMANTYL ESTERS OF UNSATURATED ACIDS 2010
  • Butov Gennadij Mikhajlovich
  • Pastukhova Natal'Ja Petrovna
  • Kamneva Ekaterina Aleksandrovna
RU2448950C1
METHOD FOR PREPARING ADAMANTYL-CONTAINING DERIVATIVES OF NAPHTHALENE 2006
  • Butov Gennadij Mikhajlovich
  • Kamneva Ekaterina Aleksandrovna
  • Mokhov Vladimir Mikhajlovich
RU2309933C1
METHOD OF PRODUCING 1-AZIDOADAMANTANE 2014
  • Butov Gennadij Mikhajlovich
  • Mokhov Vladimir Mikhajlovich
  • Burmistrov Vladimir Vladimirovich
  • Pitushkin Dmitrij Andreevich
RU2551683C1
METHOD OF PREPARING 1-(4-R-ARYL)ADAMANTANES AND DERIVATIVES THEREOF 2006
  • Butov Gennadij Mikhajlovich
  • Mokhov Vladimir Mikhajlovich
RU2307116C1

RU 2 551 682 C1

Authors

Butov Gennadij Mikhajlovich

Mokhov Vladimir Mikhajlovich

Burmistrov Vladimir Vladimirovich

Pitushkin Dmitrij Andreevich

Dates

2015-05-27Published

2014-04-22Filed