METHOD OF PRODUCING 1-ADAMANTYL ISOCYANATE Russian patent published in 2015 - IPC C07C263/00 C07C265/10 

Abstract RU 2551681 C1

FIELD: chemistry.

SUBSTANCE: method includes reacting an adamantane derivative with an isocyanate derivative in a solvent medium and then extracting the reaction product. The adamantane derivative used is 1,3-dehydroadamantane and the isocyanate derivative is a solution of isocyanic acid solution in diethyl ether prepared in advance. The reaction is carried out while heating to 30-35°C for 3 hours in a medium of diethyl ether with molar ratio of 1,3-dehydroadamantane:isocyanic acid:diethyl ether=1:1.5:20.

EFFECT: method enables to obtain 1-adamantyl isocyanate in mild conditions with high output.

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RU 2 551 681 C1

Authors

Butov Gennadij Mikhajlovich

Mokhov Vladimir Mikhajlovich

Burmistrov Vladimir Vladimirovich

Pitushkin Dmitrij Andreevich

Dates

2015-05-27Published

2014-04-22Filed