METHOD OF PRODUCING 1-AZIDOADAMANTANE Russian patent published in 2015 - IPC C07C247/14 

Abstract RU 2551683 C1

FIELD: chemistry.

SUBSTANCE: method includes reacting an adamantane derivative with an inorganic azide in a solvent. The adamantane derivative used is 1,3-dehydroadamantane and the inorganic azide is an anhydrous hydrogen azide solution in diethyl ether obtained in advance. The process takes place in diethyl ether at 20-40°C and molar ratio of 1,3-dehydroadamantane:hydrogen azide of 1:2-2.7, for 10-20 minutes.

EFFECT: method enables to obtain a 1-azidoadamantane in mild conditions with high output.

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RU 2 551 683 C1

Authors

Butov Gennadij Mikhajlovich

Mokhov Vladimir Mikhajlovich

Burmistrov Vladimir Vladimirovich

Pitushkin Dmitrij Andreevich

Dates

2015-05-27Published

2014-04-22Filed