FIELD: chemistry.
SUBSTANCE: invention relates to a method for obtaining 2,7-dicycloalkyl-2,3a,5a,7,8a,10a-hexaazaperhydropyrenes of general formula (1): 
R=cyclo-C3H5, cyclo-C5H9, cyclo-C6H11, cyclo-C5H9O, cyclo-C7H13, cyclo-C8H15, norbornyl-, wherein 1,3,5-tricycloalkyl-1,3,5-triazines where R is as pointed above are reacted with 1,4,5,8-tetraazadecalin in methanol medium in the presence of NiCl2 at a molar ratio of 1,3,5-tricycloalkyl-1,3,5-triazine:1,4,5,8-tetraazadecalin:NiCl2=2:1:(0.03-0.07) at ambient (~20°C) temperature and atmospheric pressure for 2.5-3.5 h.
EFFECT: obtaining the mentioned compound with high yield.
1 tbl, ex 11
| Title |
Year |
Author |
Number |
| METHOD OF PRODUCING 2,7-DICYCLOALKYL-4,9-DIMETHYL-2,3A,5A,7,8A,10A-HEXAAZAPERHYDROPYRENES |
2017 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
- Kutepov Boris Ivanovich
|
RU2688221C2 |
| METHOD FOR COMBINED PRODUCTION OF 2,7-DIALKYL-4,9(10)-DIMETHYL-2,3A,5A,7,8A,10A-HEXAAZAPERHYDROPYRENES |
2017 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
- Kutepov Boris Ivanovich
|
RU2688220C2 |
| METHOD OF PRODUCING 2,7-BIS-ARYL(HETARYL)SUBSTITUTED 4,9-DIMETHYL-2,3A,5A,7,8A,10A-HEXAAZAPERHYDROPYRENES |
2018 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
|
RU2703540C2 |
| METHOD OF PRODUCING 2,8-BIS-CYCLOALKYL-2,3,8,9,12C,12D-HEXAHYDRO-1H,7H-5,11-DIOXA-2,3A,4,6,6B,8,9A,10,12,12B-DECA-CYCLOCAPENTA[E,L]PYRENES |
2018 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Dyakonov Vladimir Anatolevich
- Dzhemileva Lilya Useinovna
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
|
RU2696778C1 |
| METHOD OF OBTAINING 2,7-DIALKYL-2,3a,5a,7,8a,10a-HEXAAZAPERHYDROPYRENES |
2014 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Ismagilov Rinat Arfikovich
|
RU2561506C1 |
| METHOD FOR MANUFACTURING OF IMIDOAMINE BIS-ADDUCT OF MALEOPIMARIC ACID METIL ESTER WITH DIMETHYL-HEXAAZAPERHYDROPYRENE SPACER AND ITS USE AS A DRUG WITH CYTOTOXIC ACTIVITY |
2023 |
- Rakhimova Elena Borisovna
- Kirsanov Viktor Iurevich
|
RU2794743C1 |
| METHOD OF PRODUCING 2,8-BIS-(4-HYDROXYPHENYL, 4-CARBOXYPHENYL)-2,3,8,9,12C,12D-HEXAHYDRO-1H,7H-5,11-DIOXA-2,3A,4,6,6B,8,9A,10,12,12B-DECAAZADICYCLOPENTA[E,L]PYRENES |
2019 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
|
RU2736378C1 |
| 2,8-BIS-(5-METHYLISOXAZOL-3-YL OR 1,5-DIMETHYL-3-OXO-2-PHENYL-1,2-DIHYDRO-3H-PYRAZOL-4-YL)-2,3,8, 9,12c,12d-HEXAHYDRO-1H,7H-5,11-DIOXA-2,3a.4,6,6b8,9a,10,12,12b-DECAAZADICYCLOPENTA[e,l]PYRENES, METHOD FOR THEIR PRODUCTION AND APPLICATION IN AS A PRODUCT WITH CYTOTOXIC ACTIVITY |
2021 |
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
- Dzhemileva Lilya Useinovna
- Dyakonov Vladimir Anatolevich
|
RU2785543C1 |
| METHOD OF PRODUCING 12-CYCLOALKYL-12,13,13B,13C-TETRAHYDRO-6H,11H,14H-4B,5A,10B,12,13A-PENTAAZADIBENZO[A,H]CYCLOHEPTA[1,2,3,4-DEF]FLUORENES |
2020 |
- Dzhemilev Usein Memetovich
- Ibragimov Askhat Gabdrakhmanovich
- Rakhimova Elena Borisovna
- Kirsanov Viktor Yurevich
|
RU2735740C1 |
| MALEOPIMARIC ACID METHYL ESTER IMIDOAMINE BIS-ADDUCTS WITH AZAPOLYCYCLIC SPACERS AND METHOD FOR THEIR PREPARATION |
2022 |
- Rakhimova Elena Borisovna
- Kirsanov Viktor Iurevich
|
RU2792569C1 |
