FIELD: chemistry.
SUBSTANCE: device contains a reactor closed with a lid at the top consisting of two parts as an upper cylindrical part with a workspace for the recovery of gaseous titanium tetrachloride with molten aluminium, atomized stream of inert gas, and a lower conical part for collecting and producing the recovery products in the form of powder of titanium and excess aluminium. The device is also equipped with nozzles for feeding molten aluminium and means of sputtering a gas stream, located at the top of the reactor and adopted to work in a synchronized pulse mode, a striker for crushing dispersed droplets of molten aluminium, placed near and below the nipple for the output of aluminium trichloride gas mixture, residual titanium tetrachloride and excess inert gas and placed at the bottom of the reactor for the introduction of gaseous titanium tetrachloride to the workspace, and a shut-off device for the release of titanium powder and excess aluminium from the reactor.
EFFECT: ecological purity of production in the continuous or periodic mode of operation of the device.
2 dwg
Authors
Dates
2018-01-23—Published
2016-04-19—Filed