METHOD FOR GRAPHENE PRODUCTION Russian patent published in 2018 - IPC C01B32/192 B82B3/00 B82Y40/00 

Abstract RU 2657504 C2

FIELD: chemistry.

SUBSTANCE: invention relates to chemical industry and nanotechnology. Crystalline graphite is treated with solution of ammonium persulfate in sulfuric acid, which does not contain free water. Resulting intercalated graphite compound is maintained until its expansion. Then they are hydrolyzed, washed with water and dispersed by ultrasound in an aqueous solution of surfactants, which use a mixture of oligomeric compounds containing cumulative double carbon-carbon bonds and amino groups, as well as hydroxyl groups-aminocumulene, at a mass ratio of aminocumulene: graphene of 0.25:1 to 4:1.

EFFECT: invention allows to increase efficiency of exfoliation, to increase the allowable working concentration of graphene when it is dispersed.

1 cl, 2 dwg, 3 ex

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RU 2 657 504 C2

Authors

Tkachev Aleksej Grigorevich

Melezhik Aleksandr Vasilevich

Memetov Nariman Rustemovich

Osipov Aleksej Aleksandrovich

Dates

2018-06-14Published

2016-09-16Filed