METHOD OF PRODUCING SOLKETAL Russian patent published in 2018 - IPC C07D317/20 C07D317/00 C07D319/06 

Abstract RU 2668987 C1

FIELD: technological processes.

SUBSTANCE: invention describes a method for producing a solketal which comprises reacting glycerol with an excess of acetone under acid catalysis conditions, including removing water using molecular sieves, then separating the desiccant, neutralizing the solution and distilling off acetone, while using a 6-18-fold molar excess of acetone with respect to glycerin, the process is carried out at room temperature in a medium that does not contain hydrophobic agents.

EFFECT: technical result consists in obtaining the product in high yield and with high purity.

4 cl, 1 tbl, 2 dwg

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RU 2 668 987 C1

Authors

Varfolomeev Sergej Dmitrievich

Makarov Gennadij Grigorevich

Voleva Violetta Borisovna

Komissarova Nona Lvovna

Malkova Anastasiya Vladimirovna

Ovsyannikova Margarita Nikolaevna

Koverzanova Elena Vitalevna

Usachev Sergej Valerevich

Ajnullov Tagir Samigullovich

Shamsullin Ajrat Insafovich

Ksenofontov Denis Valentinovich

Tkach Rustem Sergeevich

Dates

2018-10-05Published

2017-11-01Filed