METHODS FOR PRODUCING ORGANOPHOSPHORUS COMPOUNDS Russian patent published in 2020 - IPC C07F9/6574 

Abstract RU 2733459 C2

FIELD: chemical or physical processes.

SUBSTANCE: present invention relates to a method of purifying a solid organophosphite compound and can be used in chemical industry. Disclosed method comprises: (a) obtaining a solid organophosphite compound, subjected to recrystallization or trituration into a powder, wherein said solid organophosphite compound contains phosphorous acid; (b) dissolving said solid organophosphite compound in a hydrocarbon solvent, wherein said hydrocarbon solvent contains an aromatic hydrocarbon, a saturated aliphatic hydrocarbon or mixture thereof; and (c) removing undissolved phosphorous acid from solution, wherein content of acid in organophosphite after step (c) is 30 ppm or less, wherein said undissolved phosphorous acid is removed by filtration and/or centrifugation.

EFFECT: disclosed is a novel method which enables to efficiently purify a solid organophosphite compound from phosphorous acid.

9 cl, 18 ex, 9 tbl

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RU 2 733 459 C2

Authors

Bigi Marinus A.

Brammer Majkl A.

Miller Glenn A.

Dates

2020-10-01Published

2016-09-07Filed