METHOD AND APPARATUS FOR CLEANING CONDENSER HEAT EXCHANGERS FROM DEPOSITED PHTHALIC ANHYDRIDE Russian patent published in 2022 - IPC F28G9/00 

Abstract RU 2785182 C2

FIELD: cleaning.

SUBSTANCE: invention relates to the chemical and paint and varnish industry and is intended for intensifying production processes executed at alkyd resin synthesis units. In the production of alkyd resins, heat exchanger tubes accumulate deposits of phthalic anhydride. Cleaning, i.e., washing of tubular condenser heat exchangers, is performed by pumping the reaction mass at a temperature of 220 to 240°C through the inter-tube space of the condenser heat exchangers for an hour, allowing all the tubes and contents thereof to be warmed up, followed by washing off the entire reaction mass into the reactor. To implement the method, the unit for cleaning condenser heat exchangers from deposited phthalic anhydride is equipped with additional jumpers. The unit is equipped with additional tubular jumpers with gates between the reaction mass circulation pipeline and the jackets of the condenser heat exchangers, the jumpers are equipped with sliding gates at the inlet and outlet. The reaction mass at a temperature of 220 to 240°C enters the jackets, heats the tubes, and melts the phthalic anhydride deposited therein. The molten phthalic anhydride is washed out by the reaction mass supplied through the tubes as a washing liquid through the additional tubular bridges, followed by being washed off into the reactor and processed. The entire washing process is implemented without disassembling or cooling the unit, without stopping the production process, by redistributing the flow of the reaction mass by means of controlling the flow by means of the sliding gates placed on the jumpers, additionally installed between the reaction mass circulation pipeline and the jackets of the condenser heat exchangers.

EFFECT: complete cleaning is performed, since everything deposited in the tubes is returned to the reactor and reprocessed.

2 cl, 1 dwg

Similar patents RU2785182C2

Title Year Author Number
METHOD FOR SYNTHESIS OF ALKYD RESINS 2020
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2768758C2
METHOD FOR AUTOMATIC REGULATION OF THE POLYCONDENSATION PROCESS IN PRODUCTION OF ALKYD RESINS 2020
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2763336C1
INSTALLATION FOR ALKYD RESIN SYNTHESIS 2020
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2780510C2
METHOD AND DEVICE FOR CONTROL OF THE STAGE OF TRANSETERIFICATION IN THE PRODUCTION OF ALKYD RESINS BY ELECTROPHYSICAL METHODS OF ANALYSIS 2022
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
  • Dubovik Ekaterina Nikolaevna
RU2795748C1
METHOD FOR CONTROLLING STAGE OF TRANSESTERIFICATION IN PRODUCTION OF ALKYD VARNISHES 2017
  • Dubovik Nikolaj Sergeevich
  • Dubovik Sergej Anatolevich
  • Kozlov Evgenij Ivanovich
  • Myatyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2668365C1
METHOD OF CONTROLLING POLYCONDENSATION IN THE PRODUCTION OF ALKYD RESINS AND A DEVICE FOR REALIZING SAID METHOD 2018
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2686380C1
METHOD OF CONTROLLING POLYCONDENSATION STEP IN PRODUCTION OF ALKYD VARNISHES 2017
  • Dubovik Nikolaj Sergeevich
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2697032C2
METHOD FOR CONTROL BY HIGH-FREQUENCY TITRATION OF THE POLYCONDENSATION STAGE IN THE PRODUCTION OF ALKYD LACQUERS 2020
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2761414C1
METHOD FOR CONTROL BY ELECTROPHYSICAL METHODS OF ANALYSIS OF POLYCONDENSATION STAGE IN THE PRODUCTION OF ALKYD LACQUERS 2019
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Dubovik Nikolaj Sergeevich
  • Matyas Darya Sergeevna
  • Pichugina Irina Nikolaevna
RU2755379C2
METHOD OF PRODUCTION OF PENTAFTAIL ALKYDE RESIN 2017
  • Dubovik Nikolaj Sergeevich
  • Dubovik Sergej Antonovich
  • Kozlov Evgenij Ivanovich
  • Ivanov Ivo Vasilev
  • Matyas Darya Sergeevna
RU2644165C1

RU 2 785 182 C2

Authors

Dubovik Sergej Antonovich

Kozlov Evgenij Ivanovich

Dubovik Nikolaj Sergeevich

Matyas Darya Sergeevna

Pichugina Irina Nikolaevna

Dates

2022-12-05Published

2021-03-30Filed