FIELD: chemistry.
SUBSTANCE: method for obtaining a new compound, namely triiodide N,N-dimethylhydrazine formulas, which can be used for the synthesis of iodine-containing drugs. The method consists in the interaction of glyoxal dimethylhydrazone with bromomalonnitrile and potassium iodide in an aqueous dioxane solution. Preferably, the reaction is carried out at room temperature for 72 hours, or by heating to 40°C for 5 minutes, or under the action of ultrasound with a frequency of 90-100 Hz or microwave radiation of 150 W.
EFFECT: method for obtaining iodine-containing drugs.
2 cl, 4 ex
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Authors
Dates
2023-08-24—Published
2023-02-09—Filed