METHOD OF PRODUCING TUNGSTEN HEXAFLUORIDE Russian patent published in 2024 - IPC C01G41/04 C23C4/123 C23C16/30 C23C16/44 

Abstract RU 2830120 C1

FIELD: chemical or physical processes.

SUBSTANCE: invention relates to a method of producing tungsten hexafluoride in gas phase. Fluorination of tungsten is carried out in a vertically oriented reactor. Said reactor provides continuous downward flow of carrier gas and continuous uniform supply of tungsten wire from above inside said reactor into heating area by means of inductor high-frequency electromagnetic field. Then a drop of melted tungsten is formed at the end of the tungsten wire, from which tungsten is evaporated in the high-frequency electromagnetic field of the inductor, and tungsten nanoparticles are condensed. Then, condensed tungsten nanoparticles are carried away from the condensation zone into the reaction zone. Reagent gas in form of fluorine is introduced into said reaction zone, and tungsten nanoparticles react with fluorine to obtain tungsten hexafluoride in gas phase. Obtained tungsten hexafluoride together with the carrier gas flow is directed to the pre-cooling area. Then, tungsten hexafluoride is condensed from the carrier gas flow into cylinders-condensers.

EFFECT: obtaining tungsten hexafluoride in gas phase with purity of not less than 99_99 % in continuous mode.

3 cl, 1 dwg, 3 ex

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RU 2 830 120 C1

Authors

Vorotyntsev Andrej Vladimirovich

Kapinos Aleksandr Aleksandrovich

Markov Artem Nikolaevich

Suvorov Sergej Sergeevich

Barysheva Aleksandra Vladimirovna

Petukhov Anton Nikolaevich

Dokin Egor Sergeevich

Grachev Pavel Petrovich

Emelyanov Artem Vladimirovich

Dates

2024-11-13Published

2023-11-29Filed