FIELD: inorganic synthesis; preparation of heteropolyacids of formula: H8-m+nXm+M12-nVnO40, wherein X is P, Si, Al, Fe; M=Mo, W; n=0-6. SUBSTANCE: molybdenum or tungsten oxides or compound of general formula: M12-nVnOm, wherein M= Mo, W; n=1-6; m=33-35.5. Mixture of original element oxides is subjected to mechanical and chemical activation and the resulting products are subsequently treated with water or hydrogen peroxide at 25-100 C. EFFECT: more efficient preparation process. 4 cl
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Authors
Dates
1997-03-27—Published
1992-06-15—Filed