METHOD OF PREPARING 1-HYDROXYADAMANTANE Russian patent published in 1999 - IPC

Abstract RU 2125037 C1

FIELD: synthesis of adamantane, more particularly synthesis of biologically active compounds. SUBSTANCE: hydroxyadamantane is prepared by oxidation of adamantane in sulfuric and nitric acids on heating. Oxidation is carried out in the presence of activating methylene- acetonitrile system at molar ratio of adamantane, nitric and sulfuric acids, acetonitrile and methylene chloride of 1: 0.86-11.86-7.11: 0.19-0.24: 8.46-6.35. EFFECT: more efficient preparation method. 8 ex, 1 tbl

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RU 2 125 037 C1

Authors

Butenko L.N.

Ushchenko V.P.

Voloboev S.N.

Kalashnikov I.V.

Novakov I.A.

Dates

1999-01-20Published

1997-10-08Filed