FIELD: technological processes.
SUBSTANCE: invention may be used in chemical industry. Polycrystalline silicon is produced by blowdown and thermal conversion of silanes inside silicon tubular element heated up to temperature of 750°C ÷ 1000°C. Internal volume of tubular element that corresponds in size to heating zone is filled with porous medium made of compacted silicon fragments in the form of needles or fibers having cross section diametre from 10 to 200 µm. Density of tube internal volume filling with needle fragments prior to blowdown of silanes makes 10 ÷ 60%. Dislocation of silanes inside tubular element filled with silicon fragments is realised until tube internal volume density increases - from initial one to 85 ÷ 90%.
EFFECT: increased efficiency of silicon deposit in process of silanes pyrolysis, reduced energy intensity of this process.
3 cl, 2 tbl, 1 ex
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METHOD FOR PREPARATION OF POLYCRYSTALLINE HIGH-PURITY SILICON AND DEVICE THEREOF (VERSIONS) | 2006 |
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Authors
Dates
2009-06-10—Published
2007-06-21—Filed