METHOD OF PRODUCING 1,3-DI(R-THIO)ADAMANTANES Russian patent published in 2012 - IPC C07C319/18 C07C321/28 

Abstract RU 2448955 C1

FIELD: chemistry.

SUBSTANCE: invention relates to the chemistry of adamantane derivatives, specifically to a method of producing 1,3-di(R-thio)adamantanes of general formula: , where (1); (2); (3). The method involves binding disulphides to 1,3-dehydroadamantane, said disulphides being selected from: diphenyl sulphide, n,n'-bis-(4-bromophenyl)disulphide, n,n'-bis-(4-aminophenyl)-disulphide with molar ratio of reactants equal to 1:1.1, in a melt of the initial disulphide at temperature 100-110°C or in benzene at 80°C for 2-9 hours.

EFFECT: method of producing novel 1,3-di(R-thio)adamantanes, which enables to obtain compounds of the disclosed structural formula with sufficiently high output.

1 cl, 3 ex

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RU 2 448 955 C1

Authors

Butov Gennadij Mikhajlovich

Mokhov Vladimir Mikhajlovich

Tsapkova Julija Vladimirovna

Ivankina Ol'Ga Mikhajlovna

Zyk Nikolaj Vasil'Evich

Antipin Roman L'Vovich

Gavrilova Anna Jur'Evna

Dates

2012-04-27Published

2011-02-01Filed