FIELD: chemistry.
SUBSTANCE: invention relates to method of obtaining 3-(m-,p-methylphenyl)-tetrahydro-2H,6H-1,5,3-dithiazocenes, which cam be applied as antibacterial, antifungal and antiviral agents, as complexing agents, selective sorbents and extractants of precious metals, special reagents for suppression of vital activity of bacteria in various technical media. Essence of method lies in preliminary mixing of formaldehyde with 1,3-propanedithiol with further addition of m-, n-methylaniline and mixing at temperature ~20°C and atmospheric pressure for 4-8 hours. Output of 3-(m-,p-methylphenyl)-tetrahydro-2H,6H-1,5,3-dithiazocenes (1) constitutes 68-92%.
EFFECT: method improvement.
1 tbl, 1 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF OBTAINING 3-(o-,m-,p-NITROPHENYL)-TETRAHYDRO-2H,6H-1,5,3-DITHIAZOCENES | 2011 |
|
RU2467002C1 |
METHOD OF OBTAINING 3-(o-,m-,p-METHOXYPHENYL)-TETRAHYDRO-2H, 6H-1, 5, 3-DITHIAZOCENES | 2011 |
|
RU2467001C1 |
METHOD OF OBTAINING 3-ARYL-TETRAHYDRO-2H,6H-1,5,3-DITHIAZOCINES | 2011 |
|
RU2467000C1 |
METHOD OF OBTAINING 3-ARYL-1,5,3-DITHIAZOCANES | 2013 |
|
RU2536408C2 |
METHOD FOR PREPARING 3-(m-, p-METHYLPHENYL)-TETRAHYDRO-2H-1,5,3-DIOXAZEPINES | 2011 |
|
RU2490263C2 |
METHOD FOR PREPARING 3-(o-, m-, n-NITROPHENYL)-TETRAHYDRO-2H-1,5,3-DIOXAZEPINES | 2011 |
|
RU2490262C2 |
METHOD FOR PREPARING 3-(m-, p-METHYLPHENYL)-1,5,3-DITHIAZEPANES | 2011 |
|
RU2478625C2 |
METHOD OF PRODUCING 3-(o-,m-,n-METHOXYPHENYL)-TETRAHYDRO-2H-1,3,3-DIOXAZEPINES | 2011 |
|
RU2478096C2 |
METHOD OF OBTAINING 3-HETARYL-1,5,3-DITHIAZOCINANES | 2012 |
|
RU2536261C2 |
METHOD FOR PREPARING 2- AND 4-(1,5,3-DITHIAZOCYNAN-3-YL)PHENOLS | 2011 |
|
RU2478627C2 |
Authors
Dates
2012-11-20—Published
2011-05-30—Filed