METHOD OF OBTAINING 3-(m-,p-METHYLPHENYL)-TETRAHYDRO-2H,6H-1,5,3-DITHIAZOCENES Russian patent published in 2012 - IPC C07D285/38 

Abstract RU 2467003 C1

FIELD: chemistry.

SUBSTANCE: invention relates to method of obtaining 3-(m-,p-methylphenyl)-tetrahydro-2H,6H-1,5,3-dithiazocenes, which cam be applied as antibacterial, antifungal and antiviral agents, as complexing agents, selective sorbents and extractants of precious metals, special reagents for suppression of vital activity of bacteria in various technical media. Essence of method lies in preliminary mixing of formaldehyde with 1,3-propanedithiol with further addition of m-, n-methylaniline and mixing at temperature ~20°C and atmospheric pressure for 4-8 hours. Output of 3-(m-,p-methylphenyl)-tetrahydro-2H,6H-1,5,3-dithiazocenes (1) constitutes 68-92%.

EFFECT: method improvement.

1 tbl, 1 ex

Similar patents RU2467003C1

Title Year Author Number
METHOD OF OBTAINING 3-(o-,m-,p-NITROPHENYL)-TETRAHYDRO-2H,6H-1,5,3-DITHIAZOCENES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Ibragimov Askhat Gabdrakhmanovich
  • Akhmetova Vnira Rakhimovna
  • Korzhova Ljubov' Fedorovna
RU2467002C1
METHOD OF OBTAINING 3-(o-,m-,p-METHOXYPHENYL)-TETRAHYDRO-2H, 6H-1, 5, 3-DITHIAZOCENES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Ibragimov Askhat Gabdrakhmanovich
  • Akhmetova Vnira Rakhimovna
  • Korzhova Ljubov' Fedorovna
RU2467001C1
METHOD OF OBTAINING 3-ARYL-TETRAHYDRO-2H,6H-1,5,3-DITHIAZOCINES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Ibragimov Askhat Gabdrakhmanovich
  • Korzhova Ljubov' Fedorovna
RU2467000C1
METHOD OF OBTAINING 3-ARYL-1,5,3-DITHIAZOCANES 2013
  • Dzhemilev Usein Memetovich
  • Ibragimov Askhat Gabdrakhmanovich
  • Khalilov Leonard Mukhibovich
  • Makhmudijarova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Mudarisova Lilija Vazilevna
RU2536408C2
METHOD FOR PREPARING 3-(m-, p-METHYLPHENYL)-TETRAHYDRO-2H-1,5,3-DIOXAZEPINES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Akhmetova Vnira Rakhimovna
  • Ibragimov Askhat Gabdrakhmanovich
  • Korzhova Ljubov' Fedorovna
RU2490263C2
METHOD FOR PREPARING 3-(o-, m-, n-NITROPHENYL)-TETRAHYDRO-2H-1,5,3-DIOXAZEPINES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Akhmetova Vnira Rakhimovna
  • Ibragimov Askhat Gabdrakhmanovich
  • Korzhova Ljubov' Fedorovna
RU2490262C2
METHOD FOR PREPARING 3-(m-, p-METHYLPHENYL)-1,5,3-DITHIAZEPANES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Akhmetova Vnira Rakhimovna
  • Ibragimov Askhat Gabdrakhmanovich
  • Korzhova Ljubov' Fedorovna
RU2478625C2
METHOD OF PRODUCING 3-(o-,m-,n-METHOXYPHENYL)-TETRAHYDRO-2H-1,3,3-DIOXAZEPINES 2011
  • Dzhemilev Usein Memetovich
  • Murzakova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Akhmetova Vnira Rakhimovna
  • Ibragimov Askhat Gabdrakhmanovich
  • Korzhova Ljubov' Fedorovna
RU2478096C2
METHOD OF OBTAINING 3-HETARYL-1,5,3-DITHIAZOCINANES 2012
  • Dzhemilev Usein Memetovich
  • Ibragimov Askhat Gabdrakhmanovich
  • Makhmudijarova Natalija Nail'Evna
  • Prokof'Ev Kirill Igorevich
  • Mudarisova Lidija Vazilevna
RU2536261C2
METHOD FOR PREPARING 2- AND 4-(1,5,3-DITHIAZOCYNAN-3-YL)PHENOLS 2011
  • Dzhemilev Usein Memetovich
  • Rakhimova Elena Borisovna
  • Vasil'Eva Inna Vladimirovna
  • Janybin Vasilij Mikhajlovich
  • Ibragimov Askhat Gabdrakhmanovich
RU2478627C2

RU 2 467 003 C1

Authors

Dzhemilev Usein Memetovich

Murzakova Natalija Nail'Evna

Prokof'Ev Kirill Igorevich

Ibragimov Askhat Gabdrakhmanovich

Akhmetova Vnira Rakhimovna

Korzhova Ljubov' Fedorovna

Dates

2012-11-20Published

2011-05-30Filed