METHOD OF OBTAINING A-SECOTRITERPENE C-3(28) MONO- AND DIAMIDES AND THEIR SECOINTERMEDIATES Russian patent published in 2014 - IPC C07C13/62 C07C231/02 C07C233/58 C07J53/00 C07J63/00 

Abstract RU 2525546 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of obtaining A-secotriterpene C-3(28) mono- and diamides and their 2,3-secointermediates by fragmentation of triterpene α-hydroxyoximes and α-ketoximes under the influence of at least one acidic dehydrating agent with chlorinating properties with formation in a reaction mixture of chloroanhydride of carbonyl(or carboxyl)-containing 2,3-secointermediate. Processing of the reaction mixture with amine leads to obtaining 2,3-secotriterpene amide. A-secotriterpene C-3(28) mono- and diamindes are obtained by simplified technology.

EFFECT: reduction of expenditures for their synthesis and considerable increase of the target product output.

2 cl, 1 tbl, 18 ex

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Authors

Grishko Viktorija Viktorovna

Tolmacheva Irina Anatol'Evna

Krajnova Gul'Naz Faizovna

Nazarov Aleksej Vital'Evich

Dates

2014-08-20Published

2013-05-06Filed