METHOD FOR MANUFACTURING SPHEROIDAL ALUMINA PARTICLES Russian patent published in 2017 - IPC C01F7/02 B01J2/08 B01J32/00 B01J21/04 B01J35/10 C10G11/02 C10G35/06 C10G45/04 C10G47/12 

Abstract RU 2608775 C2

FIELD: chemistry.

SUBSTANCE: invention can be used in chemical industry. To obtain spheroidal alumina particles suspension is prepared, containing water, an acid and at least one boehmite powder. Ratio of size of crystallites along directions [020] and [120], obtained using Scherrer formula for x-ray diffraction, varies from 0.7 to 1. Method includes adding to suspension a porogenic agent, surfactant and, optionally, water or emulsion containing at least one porogenic agent, surfactant and water. Content of porogenic agent, expressed as a ratio of weight of porogenic agent to total weight of water added to obtained suspension is in range from 0.2 to 30 %. Suspension is mixed and spheroidal particles are formed by coagulation in a droplet. Obtained particles are dried and calcined. Particles have average diameter from 1.2 to 3 mm, BET specific surface area of 150–300 m2/g, value of density of filling with a seal from 0.5 to 0.6 g/ml.

EFFECT: invention enables to obtain alumina particles with high mechanical strength with low density.

15 cl, 1 dwg, 1 tbl, 11 ex

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RU 2 608 775 C2

Authors

Lakomb, Silvi

Avene, Pristsilla

Bualleg, Malika

Bazer-Bashi, Delfin

Ezen, Patrik

Lopes, Zhozef

Dates

2017-01-24Published

2012-11-16Filed