PROCESS OF OBTAINING METHYL ESTER 2-HALO-6-ALKYL-3-CYANOSUNICOTIN ACIDS Russian patent published in 2017 - IPC C07D213/79 

Abstract RU 2616980 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method for preparing methyl 2-halo-6-alkyl-3-tsianoizonikotinovyh acids of the general formula (1)

wherein R = CH3, X = Cl; R = CH3, X = Br; R = C (CH3)3, X = Cl, characterized in that the mixture consisting of 0.005 mol of 4-1,1,2,2-oksopentan tetrakarbonitrila or 5,5-dimethyl-4-1,1,2,2-oksogeksan tetrakarbonitrila 0 1 mol of methanol and 0.03 mol of concentrated hydrochloric or hydrobromic acid 0.015 mol stirred at 70-80°C to give the desired product.

EFFECT: resulting compounds can find use as microbicides and TB, antidepressants, plant protection means and as a starting material for pyridoxine.

3 ex

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RU 2 616 980 C1

Authors

Lipin Konstantin Vladimirovich

Ershov Oleg Vyacheslavovich

Nasakin Oleg Evgenevich

Dates

2017-04-19Published

2016-04-12Filed