FIELD: chemistry.
SUBSTANCE: invention relates to the field of manufacturing dispenser cathodes based on barium scandate or other materials based on barium scandate, namely, to the target material and target for physical deposition of thin films, to a dispersed cathode based on barium scandate and the method of its preparation and method of obtaining the target. The target (66) contains a mixture or consists of a mixture of barium oxide BaO, calcium oxide CaO, aluminium oxide Al2O3 and scandium oxide Sc2O3. Molar ratio of BaO:CaO:Al2O3:Sc2O3 is "b:c:x:y" while 2≤b≤5, 1≤c≤3, 2≤x+y≤b+c and 0,1≤y≤1. Way of getting the cathode includes formation of porous shell, impregnated with barium compound and scandium, obtaining intermediate layer of BaO, CaO, Al2O3 and Sc2O3. Way of getting the target includes getting a mixture of BaO, CaO, Al2O3 and Sc2O3 and sintering or melting the mixture with the formation of the target.
EFFECT: destabilizing effect reactions BaO and CaO oppose using more inert components Sc2O3 and also Al2O3, with high content of scandium oxide not only stabilizes material but with increased content of aluminium oxide improves stability.
13 cl, 3 dwg
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Authors
Dates
2017-07-03—Published
2012-07-31—Filed